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Spectroscopy - An interdisciplinary integral description of spectroscopy from UV to NMR
Peter M. Skrabal
Verlag vdf Hochschulverlag AG, 2012
ISBN 9783728133854 , 354 Seiten
Format PDF, OL
Kopierschutz Wasserzeichen
Geräte
Cover
1
Dedication
3
Imprint
6
Preface
7
Foreword
9
Content
11
1 Introduction
13
1.1 Definitions and Systematics
13
1.2 Structure_Property Relations, Synthesis, and Process Planning
14
1.3 Development of Computers, Dynamics of Analytical Methods, and Process Control
18
1.4 Economic Significance of Analytical Methods
21
1.5 On the Conception of the Book
24
2 The Electromagnetic Spectrum
27
2.1 Its Regions and Present-Day Comprehension
27
2.2 The Instrumentation
33
3 The Absorption Processes and their Energies
43
3.1 The UV and Visible Region
45
3.2 The IR and Near IR (NIR) Region
54
3.3 The ESR Region
62
3.4 The NMR Region
71
3.5 A Comparative View
97
4 The Absorption Intensities: Prerequisites and Consequences
107
4.1 The UV and Visible Region
108
4.2 The IR and Near IR (NIR) Region
117
4.3 The ESR Region
122
4.4 The NMR Region
124
4.5 A Comparative View
136
5 Spectroscopy of Analytes in the four Phases
143
5.1 The Gas Phase
144
5.2 The Liquid Phase
145
5.3 Liquid Crystalline Phases
148
5.4 Solid-State Phases
151
5.5 Sample Preparation and Sample Purity
169
5.6 Internal and External Standards
177
6 The Measuring Techniques: CW and FT Spectroscopy
181
6.1 CW Spectroscopy
181
6.2 FT Spectroscopy
185
7 Spectroscopy in Two and Three Dimensions
199
7.1 1D Pulse Sequences in NMR Spectroscopy
200
7.2 Two-Dimensional (2D) and Three-Dimensional (3D)Spectroscopy
210
8 Application Areas and Limits
219
8.1 Structure Analyses
220
8.1.1 The Positions of Absorption Bands
221
8.1.2 Scalar Couplings, NOEs, and Relaxation Times
251
8.1.3 Solid-State Spectroscopy
267
8.1.4 Two- and Three-Dimensional Spectroscopy
277
8.2 Concentration and Kinetic Measurements
283
8.3 Dynamic Aspects
296
8.4 Diffusion Measurements and Imaging Spectroscopy
306
8.5 Opt(r)odes and Sensors, Tandem or Combined Methods
317
8.6 Chemometry
320
9 The Communication of Spectroscopic Data
323
10 Literature
329
10.1 A Selection of Textbooks and Standard Works
329
10.2 My Favorite Books
330
Addendum
331
Acronym, Name, and Keyword Index
337
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